C₄₈H₆₈N₁₀O₁₆S

Base Information

• Chemical Name: C₄₈H₆₈N₁₀O₁₆S
• CAS No.: 888009-99-2
• Molecular Formula: C₄₈H₆₈N₁₀O₁₆S
• Molecular Weight: 1073.19
• Mol file: 888009-99-2.mol

Synonyms:C₄₈H₆₈N₁₀O₁₆S

Chemical Property of C₄₈H₆₈N₁₀O₁₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₆₈N₁₀O₁₆S

There total 12 articles about C₄₈H₆₈N₁₀O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(2-{2-[2-(4-{[2-(2-{2-[4-({2-[2-(2-azidoethoxy)ethoxy]ethoxy}methyl)-1H-1,2,3-triazol-1-yl]ethoxy}ethoxy)ethoxy]methyl}-1H-1,2,3-triazol-1-yl)ethoxy]ethoxy}ethyl)isoindoline-1,3-dione (888009-98-1) + 2-[2-(2-(prop-2-yn-1-yloxy)ethoxy)ethoxy]ethyl 4-methylbenzene-1-sulfonate (888009-94-7) → C48H68N10O16S (888009-99-2)

Guidance literature:

With copper; copper(II) sulfate; In tetrahydrofuran; water; at 25 ℃; for 42h;

DOI:10.1039/b518061a

Reference yield:

2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → C48H68N10O16S (888009-99-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 75 percent / NaH / tetrahydrofuran / 22 h / 0 - 25 °C

2: 87 percent / Et₃N; trimethylamine hydrochloride / acetonitrile / 1.33 h / 0 - 25 °C

3: 85 percent / Cu; CuSO₄ / tetrahydrofuran; H₂O / 20 h / 25 °C

4: 96 percent / NaN₃ / acetonitrile / 40 h / Heating

5: 80 percent / Cu; CuSO₄ / tetrahydrofuran; H₂O / 42 h / 25 °C

With sodium azide; trimethylamine hydrochloride; copper; sodium hydride; copper(II) sulfate; triethylamine; In tetrahydrofuran; water; acetonitrile;

DOI:10.1039/b518061a

Reference yield:

O-propargyl triethylene glycol (208827-90-1) → C48H68N10O16S (888009-99-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / Et₃N; trimethylamine hydrochloride / acetonitrile / 1.33 h / 0 - 25 °C

2: 85 percent / Cu; CuSO₄ / tetrahydrofuran; H₂O / 20 h / 25 °C

3: 96 percent / NaN₃ / acetonitrile / 40 h / Heating

4: 80 percent / Cu; CuSO₄ / tetrahydrofuran; H₂O / 42 h / 25 °C

With sodium azide; trimethylamine hydrochloride; copper; copper(II) sulfate; triethylamine; In tetrahydrofuran; water; acetonitrile;

DOI:10.1039/b518061a

upstream raw materials:

2-(2-{2-[2-(4-{[2-(2-{2-[4-({2-[2-(2-azidoethoxy)ethoxy]ethoxy}methyl)-1H-1,2,3-triazol-1-yl]ethoxy}ethoxy)ethoxy]methyl}-1H-1,2,3-triazol-1-yl)ethoxy]ethoxy}ethyl)isoindoline-1,3-dione

2-[2-(2-(prop-2-yn-1-yloxy)ethoxy)ethoxy]ethyl 4-methylbenzene-1-sulfonate

2-[2-(2-{2-[4-({2-[2-(2-azidoethoxy)ethoxy]ethoxy}methyl)-1H-1,2,3-triazol-1-yl]ethoxy}ethoxy)ethyl]isoindoline-1,3-dione

2-[2-(2-{2-[4-({2-[2-(2-{4-[(2-{2-[2-(4-methylbenzenesulfonyl)ethoxy]ethoxy}ethoxy)methyl]-1H-1,2,3-triazol-1-yl}ethoxy)ethoxy]ethoxy}methyl)-1H-1,2,3-triazol-1-yl]ethoxy}ethoxy)ethyl]isoindoline-1,3-dione