4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

Base Information

Chemical Name:4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester
CAS No.:1277170-42-9
Molecular Formula:C₁₄H₂₄O₃S₂Si
Molecular Weight:332.56
Hs Code.:

Synonyms:4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

Suppliers and Price of 4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

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Technology Process of 4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

There total 1 articles about 4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3753-27-3
sodium 4-methylbenzenesulfonothioate

: 119451-80-8
(chloromethoxy)(1,1-dimethylethyl)dimethylsilane

: 1277170-42-9
4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

Guidance literature:: In acetonitrile; for 4h;
DOI:10.15227/orgsyn.090.0010

Reference yield: 43.0%

: 1096711-40-8
phenyl [2-[(2R)-2-[[(tert-butyldiphenylsilyl)oxy]methyl]-4-oxopyrrolidin-1-yl]-2-oxoethyl]methylcarbamate

: 1277170-42-9
4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

: C₃₂H₄₆N₂O₅SSi₂

Guidance literature:: With sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.15227/orgsyn.090.0010

Reference yield:

: 1277170-42-9
4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester

: 1366297-65-5
(6R,8S,8aR)-8a-(([(tert-butyldimethylsilyl)oxy]methyl)sulfanyl)-6-([(tert-butyl-diphenylsilyl)oxy]methyl)-2-methyl-8-[(triethylsilyl)oxy]octahydropyrrolo[1,2-a]piperazine-1,4-dione

: 1366297-77-9
(3R,6R,8S,8aR)-3,8a-bis({[(tert-butyldimethylsilyl)oxy]methyl}sulfanyl)-6-{[(tert-butyldiphenylsilyl)oxy]methyl}-2-methyl-8-[(triethylsilyl)oxy]octahydropyrrolo[1,2-a]piperazine-1,4-dione

Guidance literature:: (6R,8S,8aR)-8a-(([(tert-butyldimethylsilyl)oxy]methyl)sulfanyl)-6-([(tert-butyl-diphenylsilyl)oxy]methyl)-2-methyl-8-[(triethylsilyl)oxy]octahydropyrrolo[1,2-a]piperazine-1,4-dione; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.0194444h;

4-methylbenzenesulfonothioic acid S-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl] ester; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Further stages;
DOI:10.1016/j.tetlet.2012.01.055