(7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone

Base Information

• Chemical Name: (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone
• CAS No.: 896137-93-2
• Molecular Formula: C₃₀H₂₁ClN₂O₆S₂
• Molecular Weight: 605.092

Synonyms:(7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone

Chemical Property of (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone

There total 6 articles about (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

7-chloro-1-(phenylsulfonyl)-1H-indole (896137-69-2) + 5-methoxy-1-phenylsulfonyl-1H-indole-2-carbonyl chloride (896137-76-1) → (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone (896137-93-2)

Guidance literature:

7-chloro-1-(phenylsulfonyl)-1H-indole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

5-methoxy-1-phenylsulfonyl-1H-indole-2-carbonyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1021/jm058033i

Reference yield:

benzenesulfonyl chloride (98-09-9) → (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone (896137-93-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 1 h / 20 °C

1.2: 72 percent / tetrahydrofuran / 1 h

2.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: 28 percent / hexane; tetrahydrofuran / -78 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;

DOI:10.1021/jm058033i

Reference yield:

7-chloro-1H-indole (53924-05-3) → (7-chloro-1-phenylsulfonyl-1H-indol-2-yl)-(5-methoxy-1-phenylsulfonyl-1H-indol-2-yl)methanone (896137-93-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 1 h / 20 °C

1.2: 72 percent / tetrahydrofuran / 1 h

2.1: n-BuLi / hexane; tetrahydrofuran / 1 h / -78 °C

2.2: 28 percent / hexane; tetrahydrofuran / -78 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;

DOI:10.1021/jm058033i

upstream raw materials:

7-chloro-1-(phenylsulfonyl)-1H-indole

5-methoxy-1-phenylsulfonyl-1H-indole-2-carbonyl chloride

7-chloro-1H-indole

5-methoxylindole

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