N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

Base Information

Chemical Name:N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester
CAS No.:113727-13-2
Molecular Formula:C₃₃H₄₆N₄O₈
Molecular Weight:626.75
Hs Code.:

Synonyms:N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

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Chemical Property of N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

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Technology Process of N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

There total 5 articles about N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1142-20-7
N-Cbz-Ala

: 113727-12-1
(2S,3S)-2-[2-((S)-2-Amino-3-tert-butoxy-propionylamino)-acetylamino]-3-methyl-pentanoic acid benzyl ester

: 113727-13-2
N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; for 20h; Ambient temperature;

Reference yield:

: 16652-75-8
L-isoleucine benzyl ester tosylate

: 113727-13-2
N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / triethylamine, EEDQ / CH₂Cl₂ / 41 h

2: CF₃COOH / CH₂Cl₂ / 1 h / Ambient temperature

3: 89 percent / EEDQ / CH₂Cl₂ / 36 h / Ambient temperature

4: morpholine / 1 h / Ambient temperature

5: 93 percent / EEDQ / CH₂Cl₂ / 20 h / Ambient temperature

With morpholine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 113727-10-9
Glycyl-L-isoleucin-benzylester

: 113727-13-2
N-(Benzyloxycarbonyl)-L-alanyl-3-O-tert-butyl-L-seryl-glycyl-L-isoleucin-benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / EEDQ / CH₂Cl₂ / 36 h / Ambient temperature

2: morpholine / 1 h / Ambient temperature

3: 93 percent / EEDQ / CH₂Cl₂ / 20 h / Ambient temperature

With morpholine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane;