Technology Process of C36H42ClN5O7
There total 8 articles about C36H42ClN5O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C
1.2: 1 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 20 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -55 °C
3.2: 1 h / -55 - 0 °C
4.1: magnesium sulfate / dichloromethane / 72 h / 20 °C
5.1: sodium tetrahydroborate / methanol / 1 h / 0 °C
With
sodium tetrahydroborate; oxalyl dichloride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
3.1: |Swern Oxidation;
DOI:10.1016/j.ejmech.2012.10.026
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
1.2: 1 h / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -55 °C
2.2: 1 h / -55 - 0 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C
4.1: magnesium sulfate / dichloromethane / 72 h / 20 °C
5.1: sodium tetrahydroborate / methanol / 1 h / 0 °C
With
sodium tetrahydroborate; oxalyl dichloride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
2.1: |Swern Oxidation;
DOI:10.1016/j.ejmech.2012.10.026
