6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

Base Information

Chemical Name:6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate
CAS No.:1416574-57-6
Molecular Formula:C₃₆H₄₀ClN₅O₇
Molecular Weight:690.196
Hs Code.:

Synonyms:6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

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Chemical Property of 6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

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Technology Process of 6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

There total 7 articles about 6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107-10-8,42939-71-9
propylamine

: 1416574-47-4
C₃₃H₃₃ClN₄O₈

: 1416574-57-6
6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1016/j.ejmech.2012.10.026

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 1416574-57-6
6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 1 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -55 °C

3.2: 1 h / -55 - 0 °C

4.1: magnesium sulfate / dichloromethane / 72 h / 20 °C

With oxalyl dichloride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide; 3.1: |Swern Oxidation;
DOI:10.1016/j.ejmech.2012.10.026

Reference yield:

: 477-67-8
picropodophyllic acid

: 1416574-57-6
6-(6-chloropurin-9-yl)hexyl 9-deoxy-9-propylimino-α-apopicropodophyllate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 1 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -55 °C

2.2: 1 h / -55 - 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C

4.1: magnesium sulfate / dichloromethane / 72 h / 20 °C

With oxalyl dichloride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide; 2.1: |Swern Oxidation;
DOI:10.1016/j.ejmech.2012.10.026