2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide

Base Information

• Chemical Name: 2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide
• CAS No.: 1026083-48-6
• Molecular Formula: C₂₂H₃₆N₆O
• Molecular Weight: 400.567

Synonyms:2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide

Chemical Property of 2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide

Chemical Property:

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Technology Process of 2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide

There total 1 articles about 2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

semicarbazide hydrochloride (563-41-7) + 4-{[2-(4-phenyl-piperazin-1-yl)-ethyl]-propyl-amino}-cyclohexanone (477788-92-4) → 2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide (1026083-48-6)

Guidance literature:

semicarbazide hydrochloride; With sodium acetate; In methanol;

4-{[2-(4-phenyl-piperazin-1-yl)-ethyl]-propyl-amino}-cyclohexanone; In methanol; for 4h; Reflux;

DOI:10.1021/jm701524h

Reference yield: 73.0%

2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide (1026083-48-6) → [2-(4-phenylpiperazin-1-yl)ethyl]propyl(4,5,6,7-tetrahydrobenzo[1,2,3]selenadiazol-6-yl)amine (874459-33-3)

Guidance literature:

With selenium(IV) oxide; acetic acid; for 0.5h;

DOI:10.1021/jm701524h

Reference yield: 69.3%

2-(4-(2-(4-phenylpiperazin-1-yl)ethyl)(propylamino)cyclohexylidene)hydrazinecarboxamide (1026083-48-6) → [2-(4-phenylpiperazin-1-yl)ethyl]propyl(4,5,6,7-tetrahydrobenzo[1,2,3]thiadiazol-6-yl)amine (874459-35-5)

Guidance literature:

With thionyl chloride; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm701524h

upstream raw materials:

semicarbazide hydrochloride

4-{[2-(4-phenyl-piperazin-1-yl)-ethyl]-propyl-amino}-cyclohexanone

Downstream raw materials:

[2-(4-phenylpiperazin-1-yl)ethyl]propyl(4,5,6,7-tetrahydrobenzo[1,2,3]thiadiazol-6-yl)amine

[2-(4-phenylpiperazin-1-yl)ethyl]propyl(4,5,6,7-tetrahydrobenzo[1,2,3]selenadiazol-6-yl)amine

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