C₄₈H₅₂N₈O₁₂S

Base Information

Chemical Name:C₄₈H₅₂N₈O₁₂S
CAS No.:1380110-97-3
Molecular Formula:C₄₈H₅₂N₈O₁₂S
Molecular Weight:965.053
Hs Code.:

C<sub>48</sub>H<sub>52</sub>N<sub>8</sub>O<sub>12</sub>S

Synonyms:C₄₈H₅₂N₈O₁₂S

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Chemical Property of C₄₈H₅₂N₈O₁₂S

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Technology Process of C₄₈H₅₂N₈O₁₂S

There total 7 articles about C₄₈H₅₂N₈O₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1380109-80-7
2-(aminomethyl)-1,5-bis(benzyloxy)-1,4-dihydropyridin-4-one

: 1380110-96-2
C₂₇H₃₄N₆O₈S

: 530-62-1
1,1'-carbonyldiimidazole

: 1380110-97-3
C₄₈H₅₂N₈O₁₂S

Guidance literature:: 2-(aminomethyl)-1,5-bis(benzyloxy)-1,4-dihydropyridin-4-one; 1,1'-carbonyldiimidazole; With triethylamine; In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.833333h;

C₂₇H₃₄N₆O₈S; In tetrahydrofuran; dichloromethane; at 20 - 25 ℃; for 19h;

Reference yield:

: 1380109-77-2
5-(benzyloxy)-1-hydroxy-2-(hydroxymethyl)pyridin-4(1H)-one

: 1380110-97-3
C₄₈H₅₂N₈O₁₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

2.1: triethylamine / dichloromethane / 1 h / 0 °C

3.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

4.1: hydrazine hydrate / ethanol / 1 h / Reflux

5.1: triethylamine / tetrahydrofuran; dichloromethane / 0.83 h / 0 °C

5.2: 19 h / 20 - 25 °C

With potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 1380110-97-3
C₄₈H₅₂N₈O₁₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: triethylamine / tetrahydrofuran; dichloromethane / 0.83 h / 0 °C

7.2: 19 h / 20 - 25 °C

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;