4-NITROBENZOYL-GLYCYL-GLYCINE

Base Information

• Chemical Name: 4-NITROBENZOYL-GLYCYL-GLYCINE
• CAS No.: 78196-53-9
• Molecular Formula: C11H11N3O6
• Molecular Weight: 281.225
• Hs Code.: 2924299090
• Mol file: 78196-53-9.mol

Synonyms:Glycine,N-[N-(4-nitrobenzoyl)glycyl]-;p-Nitrobenzoylglycylglycine;

Chemical Property of 4-NITROBENZOYL-GLYCYL-GLYCINE

Chemical Property:

• Melting Point: 218 °C
• Boiling Point: 694.1 °C at 760 mmHg
• Flash Point: 373.6 °C
• PSA: 141.32000
• Density: 1.466 g/cm³
• LogP: 0.83040

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-NITRO BENZOYL-GLYCYL-GLYCINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-NITROBENZOYL-GLYCYL-GLYCINE

There total 6 articles about 4-NITROBENZOYL-GLYCYL-GLYCINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glycylglycine (556-50-3) + 4-nitrophenyl 4-nitrobenzoate (1037-31-6) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + p-nitrobenzoylglycylglycine (78196-53-9)

Guidance literature:

In water; dimethyl sulfoxide; at 25 ℃; Rate constant;

DOI:10.1139/cjc-76-6-729

Reference yield:

glycylglycine (556-50-3) + 4-nitro-benzoyl chloride (122-04-3) → p-nitrobenzoylglycylglycine (78196-53-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1084/jem.55.5.781

Reference yield:

glycylglycine (556-50-3) + C13H7ClN2O6 (1644630-62-5) → p-nitrobenzoylglycylglycine (78196-53-9)

Guidance literature:

In water; dimethyl sulfoxide; acetonitrile; at 25 ℃; Kinetics;

DOI:10.5012/bkcs.2014.35.8.2271

upstream raw materials:

glycylglycine

4-nitro-benzoyl chloride

4-nitrophenyl 4-nitrobenzoate

2,4-dinitrophenyl p-nitrobenzoate

Downstream raw materials:

N-[N-(4-nitro-benzoyl)-glycyl]-glycine methyl ester

N-[N-(4-amino-benzoyl)-glycyl]-glycine

N-[N-(4-nitro-benzoyl)-glycyl]-glycine amide

N-[N-(4-nitro-benzoyl)-glycyl]-glycine hydrazide