2,4-dinitrophenyl 4-nitrobenzoate

Base Information

• Chemical Name: 2,4-dinitrophenyl 4-nitrobenzoate
• CAS No.: 7622-07-3
• Molecular Formula: C13H7 N3 O8
• Molecular Weight: 333.214
• Mol file: 7622-07-3.mol

Synonyms:Phenol,2,4-dinitro-, 4-nitrobenzoate (ester) (9CI); Phenol, 2,4-dinitro-,p-nitrobenzoate (ester) (8CI); 2,4-Dinitrophenyl 4-nitrobenzoate;2,4-Dinitrophenyl p-nitrobenzoate; NSC 406943; p-Nitrobenzoic acid2,4-dinitrophenyl ester

Chemical Property of 2,4-dinitrophenyl 4-nitrobenzoate

Chemical Property:

• Vapor Pressure: 3.86E-14mmHg at 25°C
• Boiling Point: 595.3°C at 760 mmHg
• Flash Point: 280.5°C
• Density: 1.599g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dinitrophenyl 4-nitrobenzoate

There total 2 articles about 2,4-dinitrophenyl 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Dinitrophenol (51-28-5) + 4-nitro-benzoyl chloride (122-04-3) → 2,4-dinitrophenyl p-nitrobenzoate (7622-07-3)

Guidance literature:

at 180 - 200 ℃;

Reference yield:

4-nitro-benzoic acid (62-23-7) → 2,4-dinitrophenyl p-nitrobenzoate (7622-07-3)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

2: NaOH / Bu₄NOH / CH₂Cl₂; H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; tetra(n-butyl)ammonium hydroxide; In dichloromethane; water;

Reference yield:

2,4-dinitrophenyl p-nitrobenzoate (7622-07-3) → 2,4-Dinitrophenol (51-28-5) + 4-nitro-benzoic acid (62-23-7)

Guidance literature:

With water; In ethanol; acetonitrile; at 24.9 - 25.1 ℃; Rate constant;

upstream raw materials:

2,4-Dinitrophenol

4-nitro-benzoyl chloride

4-nitro-benzoic acid

Downstream raw materials:

2,4-Dinitrophenol

4-nitro-benzoic acid

N-(p-nitrobenzoyl)azacyclohexane

1-morpholin-4-yl-1-(4-nitro-phenyl)-methanone