tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Base Information

Chemical Name:tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate
CAS No.:1382250-16-9
Molecular Formula:C₄₈H₆₀N₄O₉
Molecular Weight:837.026
Hs Code.:

Synonyms:tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Suppliers and Price of tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

There total 7 articles about tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1382249-89-9
(4-(benzyloxy)phenyl)(tributylstannyl)methyl methyl carbonate

: 1382250-14-7
(E)-tert-butyl 4,4'-(ethene-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

: 1382250-16-9
tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; toluene; at -25 ℃; for 1h;

Reference yield:

: 1575-37-7
4-Bromo-benzene-1,2-diamine

: 1382250-16-9
tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran / 72 h / Inert atmosphere

2: potassium phosphate / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / water; tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Microwave irradiation; sealed tube

3: boron trifluoride diethyl etherate / dichloromethane; toluene / 1 h / -25 °C

With potassium phosphate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; toluene;

Reference yield:

: 471239-60-8
di-tert-butyl (4-bromobenzene-1,2-diyl)biscarbamate

: 1382250-16-9
tert-butyl 4,4'-(3-(4-(benzyloxy)phenyl)cyclopropane-1,2-diyl)bis(benzene-4,2,1-triyl)tetracarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / water; tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Microwave irradiation; sealed tube

2: boron trifluoride diethyl etherate / dichloromethane; toluene / 1 h / -25 °C

With potassium phosphate; boron trifluoride diethyl etherate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; toluene;