2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

Base Information

Chemical Name:2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine
CAS No.:1380445-20-4
Molecular Formula:C₄₁H₃₄BN₃O₂
Molecular Weight:611.551
Hs Code.:

Synonyms:2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

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Chemical Property of 2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

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Technology Process of 2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

There total 12 articles about 2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1268251-22-4
2-[3-chloro-5-(phenanthrene-9-yl)phenyl]-4,6-diphenyl-1,3,5-triazine

: 73183-34-3
bis(pinacol)diborane

: 1380445-20-4
2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: With potassium acetate; palladium diacetate; XPhos; In 1,4-dioxane; at 100 ℃; for 4h; Inert atmosphere;

Reference yield: 81.4%

: 1268250-99-2
2-(3-bromo-5-(phenanthren-9-yl)phenyl)-4,6-diphenyl-1,3,5-triazine

: 73183-34-3
bis(pinacol)diborane

: 1380445-20-4
2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 90 ℃; for 12h;

Reference yield:

: 68572-87-2
9-phenanthrenylboronic acid

: 1380445-20-4
2-[3-{(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl}-5-(9-phenanthryl)phenyl]-4,6-diphenyl-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 4 h / 60 °C / Inert atmosphere

2: potassium acetate / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 5 h / 70 °C / Inert atmosphere

With potassium acetate; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; toluene;