tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

Base Information

Chemical Name:tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate
CAS No.:1314518-54-1
Molecular Formula:C₂₂H₁₉ClN₂O₂
Molecular Weight:378.858
Hs Code.:

Synonyms:tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

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Technology Process of tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

There total 2 articles about tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1116-98-9
cyanoacetic acid tert-butyl ester

: 10352-30-4
2,6-dichloro-4-phenylquinoline

: 1314518-54-1
tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

Guidance literature:: With sodium t-butanolate; In N,N-dimethyl-formamide; at 105 ℃; for 3h;
DOI:10.1002/ejoc.201100108

Reference yield:

: 30169-33-6
6-Chlor-1,2-dihydro-4-phenylchinolin-2-on

: 1314518-54-1
tert-butyl (2Z)-2-[6-chloro-4-phenylquinolin-2(1H)-ylidene]-2-cyanoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate

2: sodium t-butanolate / N,N-dimethyl-formamide / 3 h / 105 °C

With sodium t-butanolate; trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100108