N-phenylpropiolyl salicylhydrazide

Base Information

Chemical Name:N-phenylpropiolyl salicylhydrazide
CAS No.:960251-99-4
Molecular Formula:C₁₆H₁₂N₂O₃
Molecular Weight:280.283
Hs Code.:

Synonyms:N-phenylpropiolyl salicylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenylpropiolyl salicylhydrazide

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Technology Process of N-phenylpropiolyl salicylhydrazide

There total 1 articles about N-phenylpropiolyl salicylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

: 936-02-7
2-Hydroxybenzoylhydrazine

: 637-44-5
phenylpropyolic acid

: 960251-99-4
N-phenylpropiolyl salicylhydrazide

Guidance literature:: phenylpropyolic acid; With pivaloyl chloride; triethylamine; In chloroform; at 20 ℃; for 0.5h;

2-Hydroxybenzoylhydrazine; In chloroform; at 40 ℃; for 4h; Further stages.;
DOI:10.1021/ja075945w

Reference yield:

: 113859-74-8
Mn(CH₃COO)₂·H₂O

: 960251-99-4
N-phenylpropiolyl salicylhydrazide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: [Mn₁₅(N-phenylpropiolyl salicylhydrazide(-3H))15(H₂O)9(DMF)6]

Guidance literature:: With O₂; In N,N-dimethyl-formamide; ligand and Mn acetate mixed in DMF soln.; crystd. by layering with Et2O; single crystals obtained;
DOI:10.1021/ja075945w