ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

Base Information

Chemical Name:ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate
CAS No.:98105-65-8
Molecular Formula:C₁₈H₁₃Cl₂F₂NO₃
Molecular Weight:400.209
Hs Code.:

Synonyms:ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

Suppliers and Price of ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

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Technology Process of ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

There total 5 articles about ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: ethyl 2,4-dichloro-α-[(dimethylamino)methylene]-5-fluoro-β-oxobenzenepropanoate

: 371-40-4
4-fluoroaniline

: 98105-65-8
ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

Guidance literature:: In ethanol;
DOI:10.1021/jm070083v

Reference yield:

: 86393-34-2
2,4-dichloro-5-fluorobenzoyl chloride

: 98105-65-8
ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / N,N-diisopropylethylamine / 3 h / 85 - 90 °C

2: 51 percent / ethanol

With N-ethyl-N,N-diisopropylamine; In ethanol;
DOI:10.1021/jm070083v

Reference yield:

: 1117-37-9
ethyl (E)-3-(dimethylamino)acrylate

: 98105-65-8
ethyl 2,4-dichloro-5-fluoro-α-[[(4-fluorophenyl)amino]methylene]-β-oxobenzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / N,N-diisopropylethylamine / 3 h / 85 - 90 °C

2: 51 percent / ethanol

With N-ethyl-N,N-diisopropylamine; In ethanol;
DOI:10.1021/jm070083v