Technology Process of C29H46O4S
There total 9 articles about C29H46O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: CH3CH2COOH / 145 °C
2: LiBH4 / methanol
3: 97 percent / sodium; hexamethylphosphoramide / 2-methyl-propan-2-ol
4: 89 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2
5: NaI / butan-2-one / Heating
6: dimethylformamide / 70 °C
7: 85 percent / HBF4 / methanol; H2O
8: (COCl)2; dimethyl sulfoxide; triethylamine / -78 °C
9: 96 percent / CH2Cl2 / 22 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium borohydride; tetrafluoroboric acid; oxalyl dichloride; sodium; dimethyl sulfoxide; propionic acid; triethylamine; sodium iodide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
8: Swern oxidation / 9: Wittig olefination;
DOI:10.1002/anie.200603853
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 97 percent / sodium; hexamethylphosphoramide / 2-methyl-propan-2-ol
2: 89 percent / triethylamine; 4-(dimethylamino)pyridine / CH2Cl2
3: NaI / butan-2-one / Heating
4: dimethylformamide / 70 °C
5: 85 percent / HBF4 / methanol; H2O
6: (COCl)2; dimethyl sulfoxide; triethylamine / -78 °C
7: 96 percent / CH2Cl2 / 22 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tetrafluoroboric acid; oxalyl dichloride; sodium; dimethyl sulfoxide; triethylamine; sodium iodide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;
6: Swern oxidation / 7: Wittig olefination;
DOI:10.1002/anie.200603853
