2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

Base Information

Chemical Name:2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone
CAS No.:1018524-30-5
Molecular Formula:C₁₉H₂₂N₂O₃
Molecular Weight:326.395
Hs Code.:

Synonyms:2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

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Chemical Property of 2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

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Technology Process of 2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

There total 3 articles about 2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82924-82-1
1-(6,7-Dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-2-(4-nitro-phenyl)-ethanone

: 1018524-30-5
2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00013a017

Reference yield:

: 104-03-0
4-nitrobenzeneacetic acid

: 1018524-30-5
2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 3 h / Heating

2: NaHCO₃ / acetone / 6 h / Ambient temperature

3: H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

With thionyl chloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; acetone;
DOI:10.1021/jm00013a017

Reference yield:

: 50434-36-1
4-nitrophenylacetyl chloride

: 1018524-30-5
2-(4-Amino-phenyl)-1-(6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / acetone / 6 h / Ambient temperature

2: H₂ / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; acetone;
DOI:10.1021/jm00013a017