N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

Base Information

Chemical Name:N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide
CAS No.:140660-60-2
Molecular Formula:C₃₂H₄₂N₄O₅
Molecular Weight:562.709
Hs Code.:

Synonyms:N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

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Chemical Property of N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

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Technology Process of N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

There total 2 articles about N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 20776-45-8
5-benzyloxytryptamine

: 76684-89-4
loxistatin acid

: 140660-60-2
N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

Guidance literature:: With 4-methyl-morpholine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; In tetrahydrofuran; at 0 - 20 ℃; for 25h;
DOI:10.1021/jm00089a015

Reference yield:

: 88321-09-9
aloxistatin

: 140660-60-2
N-<2-<5-(benzyloxy)-1H-indol-3-yl>ethyl> (2S,3S)-3-<<(S)-3-methyl-1-<(3-methylbutyl)carbamoyl>butyl>carbamoyl>-2-oxiranecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 5 h / 0 - 20 °C

2: 88 percent / HOBT, N-methylmorpholine, BOP-Cl / tetrahydrofuran / 25 h / 0 - 20 °C

With 4-methyl-morpholine; potassium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; benzotriazol-1-ol; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00089a015