Technology Process of C25H28O7
There total 8 articles about C25H28O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
titanium(IV) isopropylate; titanium tetrachloride;
In
toluene;
at 0 - 20 ℃;
for 1.16667h;
Large scale;
- Guidance literature:
-
With
titanium(IV) isopropylate; titanium tetrachloride;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol9016589
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Large scale
2: potassium carbonate / methanol / 3 h / 45 - 50 °C / Large scale
3: tetrahydrofuran / 17 h / 0 - 70 °C / Large scale
4: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 2 h / 0 - 30 °C / Large scale
5: (DHQ)2AQN; potassium hexacyanoferrate(III); potassium carbonate; potassium osmate(VI) dihydrate / butan-1-ol; water / 18 h / -5 - 0 °C / Large scale
6: 4-methyl-morpholine; dmap / toluene / 6 h / 5 - 75 °C / Large scale
7: titanium tetrachloride; titanium(IV) isopropylate / toluene / 1.17 h / 0 - 20 °C / Large scale
With
4-methyl-morpholine; titanium(IV) isopropylate; dmap; potassium osmate(VI) dihydrate; (DHQ)2AQN; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; butan-1-ol;
