BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER

Base Information

Chemical Name:BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER
CAS No.:50595-38-5
Molecular Formula:C28H28 O P2
Molecular Weight:442.47
Hs Code.:2909309090
Mol file:50595-38-5.mol

Synonyms:Phosphine,(oxydi-2,1-ethanediyl)bis[diphenyl- (9CI);1,5-Bis(diphenylphosphino)-3-oxapentane; Bis(2-(diphenylphosphino)ethyl) ether;[2-[2-(Diphenylphosphino)ethoxy]ethyl]diphenylphosphine

Suppliers and Price of BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
[Bis(2-diphenylphosphino)ethyl]ether, min. 98%
1g
$ 72.00

Strem Chemicals
[Bis(2-diphenylphosphino)ethyl]ether, min. 98%
25g
$ 1127.00

Strem Chemicals
[Bis(2-diphenylphosphino)ethyl]ether, min. 98%
5g
$ 283.00

Arctom
(Oxybis(ethane-2,1-diyl))bis(diphenylphosphine) 98%
1g
$ 190.00

Arctom
(Oxybis(ethane-2,1-diyl))bis(diphenylphosphine) 98%
5g
$ 620.00

American Custom Chemicals Corporation
BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER 95.00%
5MG
$ 496.54

Total 9 raw suppliers

Chemical Property of BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER

Chemical Property:

Boiling Point:554.9±35.0 °C(Predicted)
PSA：36.41000
LogP:5.26880
Sensitive.:air sensitive

Purity/Quality:

97% ^*data from raw suppliers

[Bis(2-diphenylphosphino)ethyl]ether, min. 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER

There total 2 articles about BIS(2-DIPHENYLPHOSPHINO)ETHYL ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 111-44-4
3-oxa-1,5-dichloropentane

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 50595-38-5
bis[(2-diphenylphosphino)ethyl]ether

Guidance literature:: In tetrahydrofuran; at 30 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1002/smll.201600407

Reference yield: 42.0%

: 5414-19-7
1,1'-oxybis(2-bromo-ethane)

: 829-85-6
diphenylphosphane

: 50595-38-5
bis[(2-diphenylphosphino)ethyl]ether

Guidance literature:: diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane;

1,1'-oxybis(2-bromo-ethane); In tetrahydrofuran; hexane; at -50 - 20 ℃; Further stages.;
DOI:10.1021/ja0200239

Reference yield: 94.0%

: 33677-56-4
Pt(dba)2

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 50595-38-5
bis[(2-diphenylphosphino)ethyl]ether

: 740846-59-7
platinum(O)(η2-C60)[Ph2PCH2(CH2OCH2)CH2PPh2]

Guidance literature:: In toluene; (N2) Pd:C60:L=1:1:1, C60 in toluene treated with Pd complex , stirred atroom temp. for 30 min, treated with ligand, stirred for 0.5 h; layered with hexane, standed overnight, filtered, washed (toluene), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200300513