N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

Base Information

Chemical Name:N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide
CAS No.:1051433-65-8
Molecular Formula:C₁₇H₁₄F₂N₂O₃
Molecular Weight:332.307
Hs Code.:

Synonyms:N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

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Technology Process of N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

There total 5 articles about N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 849217-48-7
((4-fluorophenyl)carbamoyl)cyclopropanecarboxylic acid

: 399-95-1
4-amino-3-fluorophenol

: 1051433-65-8
N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 25 ℃; for 16h;

Reference yield: 39.0%

: 18266-53-0
2-fluoro-4-hydroxyaniline hydrochloride

: 1051433-65-8
N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

Guidance literature:: ((4-fluorophenyl)carbamoyl)cyclopropanecarboxylic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2-fluoro-4-hydroxyaniline hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

With hydrogenchloride; sodium hydroxide; more than 3 stages;

Reference yield: 39.0%

: 18266-53-0
2-fluoro-4-hydroxyaniline hydrochloride

: 849217-48-7
((4-fluorophenyl)carbamoyl)cyclopropanecarboxylic acid

: 1051433-65-8
N-(2-fluoro-4-hydroxyphenyl)-N'-(4-fluorophenyl)cyclopropane-1,1-dicarboxamide

Guidance literature:: ((4-fluorophenyl)carbamoyl)cyclopropanecarboxylic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2-fluoro-4-hydroxyaniline hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;