octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Base Information

Chemical Name:octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside
CAS No.:367921-22-0
Molecular Formula:C₅₃H₅₈O₁₂
Molecular Weight:887.036
Hs Code.:

Synonyms:octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Suppliers and Price of octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

There total 8 articles about octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 219627-06-2
octyl 2,3-di-O-benzyl-α-D-arabinofuranoside

: 2,3-5-tri-O-benzoyl-α-D-arabinofuranosyl 2,2,2-trichloroacetimidate

: 367921-22-0
octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/S0968-0896(01)00180-8

Reference yield:

: 111-87-5
octanol

: 367921-22-0
octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: SnCl₄ / acetonitrile / 0.5 h / 0 °C

1.2: 75 percent / acetonitrile / 1.5 h / 0 - 20 °C

2.1: 86 percent / NaOMe / methanol / 5 h / 20 °C

3.1: 73 percent / pyridine / 50 °C

4.1: NaH / tetrahydrofuran / 0.25 h / 20 °C

4.2: tetrahydrofuran / 3 h / 20 °C

5.1: 2.25 g / trifluoroacetic acid / CHCl₃ / 1 h / 0 °C

6.1: 88 percent / BF₃*Et₂O / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With pyridine; boron trifluoride diethyl etherate; sodium methylate; tin(IV) chloride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1016/S0968-0896(01)00180-8

Reference yield:

: 100-39-0
benzyl bromide

: 367921-22-0
octyl 5-O-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)-2,3-di-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 0.25 h / 20 °C

1.2: tetrahydrofuran / 3 h / 20 °C

2.1: 2.25 g / trifluoroacetic acid / CHCl₃ / 1 h / 0 °C

3.1: 88 percent / BF₃*Et₂O / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With boron trifluoride diethyl etherate; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1016/S0968-0896(01)00180-8