erythro-5,6-bis(4-hydroxyphenyl)octanal

Base Information

Chemical Name:erythro-5,6-bis(4-hydroxyphenyl)octanal
CAS No.:120579-05-7
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

Synonyms:erythro-5,6-bis(4-hydroxyphenyl)octanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-5,6-bis(4-hydroxyphenyl)octanal

Chemical Property:

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Technology Process of erythro-5,6-bis(4-hydroxyphenyl)octanal

There total 4 articles about erythro-5,6-bis(4-hydroxyphenyl)octanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120578-96-3
methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

: 120579-05-7
erythro-5,6-bis(4-hydroxyphenyl)octanal

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; toluene; at -70 ℃; for 2.5h;
DOI:10.1021/jm00127a023

Reference yield:

: tert-butyl 6-hydroxy-5,6-bis(4-methoxyphenyl)octanoate

: 120579-05-7
erythro-5,6-bis(4-hydroxyphenyl)octanal

Guidance literature:: Multi-step reaction with 4 steps

1: 45.5 percent / H₂, perchloric acid / Pd/C / acetic acid / 2250.2 Torr

2: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

3: 95 percent / diethyl ether / 0.03 h

4: 63 mg / diisobutylaluminum hydride / toluene; diethyl ether / 2.5 h / -70 °C

With perchloric acid; hydrogen; boron tribromide; diisobutylaluminium hydride; palladium on activated charcoal; In diethyl ether; dichloromethane; acetic acid; toluene;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120579-05-7
erythro-5,6-bis(4-hydroxyphenyl)octanal

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / diethyl ether / 0.03 h

2: 63 mg / diisobutylaluminum hydride / toluene; diethyl ether / 2.5 h / -70 °C

With diisobutylaluminium hydride; In diethyl ether; toluene;
DOI:10.1021/jm00127a023