erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

Base Information

Chemical Name:erythro-5,6-bis(4-hydroxyphenyl)-1-nonene
CAS No.:120579-06-8
Molecular Formula:C₂₁H₂₆O₂
Molecular Weight:310.436
Hs Code.:

Synonyms:erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

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Technology Process of erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

There total 5 articles about erythro-5,6-bis(4-hydroxyphenyl)-1-nonene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 120579-05-7
erythro-5,6-bis(4-hydroxyphenyl)octanal

: 120579-06-8
erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jm00127a023

Reference yield:

: tert-butyl 6-hydroxy-5,6-bis(4-methoxyphenyl)octanoate

: 120579-06-8
erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

Guidance literature:: Multi-step reaction with 5 steps

1: 45.5 percent / H₂, perchloric acid / Pd/C / acetic acid / 2250.2 Torr

2: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

3: 95 percent / diethyl ether / 0.03 h

4: 63 mg / diisobutylaluminum hydride / toluene; diethyl ether / 2.5 h / -70 °C

5: 51 percent / potassium tert-butoxide / tetrahydrofuran / 2 h / 20 °C

With perchloric acid; potassium tert-butylate; hydrogen; boron tribromide; diisobutylaluminium hydride; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; toluene;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120579-06-8
erythro-5,6-bis(4-hydroxyphenyl)-1-nonene

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / diethyl ether / 0.03 h

2: 63 mg / diisobutylaluminum hydride / toluene; diethyl ether / 2.5 h / -70 °C

3: 51 percent / potassium tert-butoxide / tetrahydrofuran / 2 h / 20 °C

With potassium tert-butylate; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/jm00127a023