methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

Base Information

Chemical Name:methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate
CAS No.:120578-96-3
Molecular Formula:C₂₁H₂₆O₄
Molecular Weight:342.435
Hs Code.:

Synonyms:methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

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Chemical Property of methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

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Technology Process of methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

There total 3 articles about methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120578-96-3
methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

Guidance literature:: In diethyl ether; for 0.0333333h;
DOI:10.1021/jm00127a023

Reference yield:

: tert-butyl 6-hydroxy-5,6-bis(4-methoxyphenyl)octanoate

: 120578-96-3
methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 45.5 percent / H₂, perchloric acid / Pd/C / acetic acid / 2250.2 Torr

2: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

3: 95 percent / diethyl ether / 0.03 h

With perchloric acid; hydrogen; boron tribromide; palladium on activated charcoal; In diethyl ether; dichloromethane; acetic acid;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-38-4,120578-47-4,120578-48-5
(5S*,6R*)-5,6-bis(4-methoxyphenyl)-1-octanoic acid

: 120578-96-3
methyl erythro-5,6-bis(4-hydroxyphenyl)octanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

2: 95 percent / diethyl ether / 0.03 h

With boron tribromide; In diethyl ether; dichloromethane;
DOI:10.1021/jm00127a023