(2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol

Base Information

• Chemical Name: (2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol
• CAS No.: 1204595-67-4
• Molecular Formula: C₂₅H₃₄O₅
• Molecular Weight: 414.542

Synonyms:(2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol

Chemical Property of (2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol

Chemical Property:

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Technology Process of (2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol

There total 1 articles about (2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

p-Anisaldehyde dimethyl acetal (2186-92-7) + (2S,3S,4R,5S,6S)-5-(benzyloxy)-2,4,6-trimethylheptane-1,3,7-triol (171231-73-5) → (2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol (1204595-67-4)

Guidance literature:

With camphor-10-sulfonic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol9026842

Reference yield: 90.0%

(2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol (1204595-67-4) + tert-butyldimethylsilyl chloride (18162-48-6) → (((2S,3S,4S)-3-(benzyloxy)-4-((4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)-2-methylpentyl)oxy)(tert-butyl)dimethylsilane

Guidance literature:

With 1H-imidazole; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2015.12.101

Reference yield: 75.0%

(2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol (1204595-67-4) + chloromethyl methyl ether (107-30-2) → (4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan (1320344-47-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0030-1259967

upstream raw materials:

p-Anisaldehyde dimethyl acetal

(2S,3S,4R,5S,6S)-5-(benzyloxy)-2,4,6-trimethylheptane-1,3,7-triol

Downstream raw materials:

C₂₅H₃₆O₅

(2S,3S,4R,5S,6S)-5-(benzyloxy)-3-[(4-methoxybenzyl)oxy]-7-(methoxymethoxy)-2,4,6-trimethylheptan-1-ol

C₂₇H₃₈O₆

(2R,4E,6S,7S,8R,9S,10S)-9-(benzyloxy)-7-[(4-methoxybenzyl)oxy]-11-(methoxymethoxy)-2,6,8,10-tetramethyl-1-[(1,1,1-triisopropylsilyl)oxy]-4-undecen-3-one

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