(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

Base Information

Chemical Name:(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan
CAS No.:1320344-47-5
Molecular Formula:C₂₇H₃₈O₆
Molecular Weight:458.595
Hs Code.:

Synonyms:(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

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Technology Process of (4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

There total 2 articles about (4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1204595-67-4
(2S,3S,4S)-3-(benzyloxy)-4-[(4S,5S)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl]-2-methylpentan-1-ol

: 107-30-2
chloromethyl methyl ether

: 1320344-47-5
(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1259967

Reference yield:

: 171231-73-5
(2S,3S,4R,5S,6S)-5-(benzyloxy)-2,4,6-trimethylheptane-1,3,7-triol

: 1320344-47-5
(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1055/s-0030-1259967

Reference yield: 80.0%

: 1320344-47-5
(4S,5S)-4-[(1S,2S,3S)-2-(benzyloxy)-4-(methoxymethoxy)-1,3-dimethylbutyl]-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan

: 1320344-48-6
(2S,3S,4R,5S,6S)-5-(benzyloxy)-3-[(4-methoxybenzyl)oxy]-7-(methoxymethoxy)-2,4,6-trimethylheptan-1-ol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -20 - 0 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1259967