2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole
CAS No.:1338705-66-0
Molecular Formula:C₂₉H₃₀ClN₃O₅
Molecular Weight:536.027
Hs Code.:

Synonyms:2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

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Chemical Property of 2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

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Technology Process of 2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

There total 9 articles about 2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 123-75-1
pyrrolidine

: 1338705-65-9
2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(chloromethyl)-1,3,4-oxadiazole

: 1338705-66-0
2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

Reference yield:

: 1338705-62-6
C₂₇H₂₄ClNO₈

: 1338705-66-0
2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / N,N-dimethyl-formamide / 14 h / 20 °C

2: sodium hydrogencarbonate / 0.75 h / 20 °C

3: Burgess Reagent / 1,4-dioxane / 0.67 h / 120 °C

4: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

With Burgess Reagent; sodium hydrogencarbonate; potassium carbonate; hydrazine hydrate; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 1338705-63-7
2-chloro-3,4-bis((4-methoxybenzyl)oxy)benzohydrazide

: 1338705-66-0
2-(2-chloro-3,4-bis((4-methoxybenzyl)oxy)phenyl)-5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / 0.75 h / 20 °C

2: Burgess Reagent / 1,4-dioxane / 0.67 h / 120 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

With Burgess Reagent; sodium hydrogencarbonate; potassium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;