2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

Base Information

Chemical Name:2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide
CAS No.:1448816-31-6
Molecular Formula:C₃₁H₃₁NO₇
Molecular Weight:529.59
Hs Code.:

Synonyms:2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

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Chemical Property of 2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

Chemical Property:

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Technology Process of 2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

There total 10 articles about 2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-benzyloxy)-4-methoxybenzoylchloride

: 1448816-30-5
2-(benzyloxy)-3,4,5-trimethoxyaniline

: 1448816-31-6
2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 100-39-0
benzyl bromide

: 1448816-31-6
2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

2: tin(II) chloride dihdyrate / ethyl acetate / 20 h / 60 °C / Inert atmosphere

3: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

With tin(II) chloride dihdyrate; potassium carbonate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 2103-57-3
2,3,4-trimethoxybenzaldehyde

: 1448816-31-6
2-(benzyloxy)-N-(2-(benzyloxy)-3,4,5-trimethoxyphenyl)-4-methoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid / acetic acid / 1 h / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 6 h / Inert atmosphere

2.2: 4 h / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

4.1: tin(II) chloride dihdyrate / ethyl acetate / 20 h / 60 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

With tin(II) chloride dihdyrate; nitric acid; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide; 2.1: |Dakin Phenol Oxidation / 2.2: |Dakin Phenol Oxidation;
DOI:10.1016/j.bmcl.2013.06.004