(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

Base Information

Chemical Name:(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide
CAS No.:203736-27-0
Molecular Formula:C₁₇H₁₈N₂O₄
Molecular Weight:314.341
Hs Code.:

Synonyms:(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

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Technology Process of (1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

There total 2 articles about (1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.8%

: 27383-59-1
ethyl (2-hydroxyphenylcarbamoyl)formate

: 37577-28-9,58550-13-3,757124-50-8
(1S,2R)-(+)-norphedrine

: 203736-27-0
(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

Guidance literature:: In ethanol; for 12h; Heating;
DOI:10.1039/a704640e

Reference yield:

: 95-55-6
2-amino-phenol

: 203736-27-0
(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71.9 percent / tetrahydrofuran / 1 h / 25 °C

2: 61.8 percent / ethanol / 12 h / Heating

In tetrahydrofuran; ethanol;
DOI:10.1039/a704640e

Reference yield: 98.0%

: 683-18-1
dibutyltin chloride

: 203736-27-0
(1S,2R)-(-)-[N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N'-(2-hydroxy-phenyl)]oxalamide

: 1-(2',2'-dibutyl-1'-oxa-3'-aza-2'-stanna-indan-3'-yl)-2-(2'',2''-dibutyl-4''-methyl-5''-phenyl-[1,3,2]oxazastannolidin-3''-yl)ethane-1,2-dione

Guidance literature:: With (CH₃CH₂)3N; In ethanol; soln. of ligand in EtOH, (CH3CH2)3N mixed with soln. of (CH3(CH2)3)2SnCl2 in EtOH for a few min; filtered, washed with hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2005.11.072