C₂₃H₂₅N₅O₂

Base Information

Chemical Name:C₂₃H₂₅N₅O₂
CAS No.:1346243-02-4
Molecular Formula:C₂₃H₂₅N₅O₂
Molecular Weight:403.484
Hs Code.:

C<sub>23</sub>H<sub>25</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₂₃H₂₅N₅O₂

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Chemical Property of C₂₃H₂₅N₅O₂

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Technology Process of C₂₃H₂₅N₅O₂

There total 7 articles about C₂₃H₂₅N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1346133-39-8
N-(3,5-dimethoxyphenyl)-3-(1-methyl-1H-pyrazol-4-yl)-6-quinoxalinamine

: 106-94-5
propyl bromide

: 1346243-02-4
C₂₃H₂₅N₅O₂

Guidance literature:: N-(3,5-dimethoxyphenyl)-3-(1-methyl-1H-pyrazol-4-yl)quinoxaline-6-amine; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 20 ℃; for 0.5h;

propyl bromide; In tetrahydrofuran; toluene; at 20 ℃; for 3h;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346243-02-4
C₂₃H₂₅N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 2 h / 100 °C

1.2: Cooling with ice

2.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux

3.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0.5 h / 20 °C

4.2: 3 h / 20 °C

With potassium hexamethylsilazane; sodium carbonate; sodium t-butanolate; trichlorophosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; toluene;

Reference yield:

: 89891-65-6
7-bromo-2-chloroquinoxaline

: 1346243-02-4
C₂₃H₂₅N₅O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux

2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0.5 h / 20 °C

3.2: 3 h / 20 °C

With potassium hexamethylsilazane; sodium carbonate; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; toluene;