bis(dimethylketoximato)triphenylantimony(V)

Base Information

Chemical Name:bis(dimethylketoximato)triphenylantimony(V)
CAS No.:75392-01-7
Molecular Formula:C₂₄H₂₇N₂O₂Sb
Molecular Weight:497.241
Hs Code.:

Synonyms:bis(dimethylketoximato)triphenylantimony(V)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(dimethylketoximato)triphenylantimony(V)

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Technology Process of bis(dimethylketoximato)triphenylantimony(V)

There total 1 articles about bis(dimethylketoximato)triphenylantimony(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 603-36-1
triphenylantimony

: 127-06-0
acetone oxime

: 75392-01-7
bis(dimethylketoximato)triphenylantimony(V)

Guidance literature:: With (CH₃)3COOH; In hexane; byproducts: (CH3)3COH, H2O; addn. of a soln. of peroxide in hexane to a soln. of antimony compd. andligand in hexane with stirring during 20 min, keeping at 20°C fo r 2 h; sepn. of ppt., washing with hexane, drying; elem. anal.;
DOI:10.1023/A:1019634307064

Reference yield: 53.0%

: 75392-01-7
bis(dimethylketoximato)triphenylantimony(V)

: 603-36-1
triphenylantimony

Guidance literature:: byproducts: dimethyl ketoxime; heated at 170-230°C/0.4 Hgmm; products are distd. out, Sb-compd. crystd. by addn. of Ph3Sb crystal;

upstream raw materials:

triphenylantimony

acetone oxime