2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Base Information

Chemical Name:2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal
CAS No.:615249-48-4
Molecular Formula:C₂₄H₂₅NO₈
Molecular Weight:455.464
Hs Code.:

Synonyms:2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Suppliers and Price of 2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

There total 3 articles about 2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 108-24-7
acetic anhydride

: 228399-13-1
2,5-anhydro-4-azido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

: 615249-48-4
2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Guidance literature:: With platinum(IV) oxide; hydrogen; acetic acid; at 20 ℃; for 21h;
DOI:10.1016/j.ejmech.2019.111712

Reference yield:

: 98-88-4
benzoyl chloride

: 615249-48-4
2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / dimethyl sulfoxide / 26 h / 108 - 112 °C

1.2: 24 h / 20 °C

2.1: acetic acid; platinum(IV) oxide; hydrogen / 21 h / 20 °C

With platinum(IV) oxide; sodium azide; hydrogen; acetic acid; In dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2019.111712

Reference yield:

: 258336-08-2
Benzoic acid (1R,2R,4R,5R)-4-[1,3]dioxolan-2-yl-3,6-dioxa-bicyclo[3.1.0]hex-2-ylmethyl ester

: 615249-48-4
2,5-anhydro-4-acetamido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / dimethyl sulfoxide / 26 h / 108 - 112 °C

1.2: 24 h / 20 °C

2.1: acetic acid; platinum(IV) oxide; hydrogen / 21 h / 20 °C

With platinum(IV) oxide; sodium azide; hydrogen; acetic acid; In dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2019.111712