N-cycloheptylbenzamide

Base Information

• Chemical Name: N-cycloheptylbenzamide
• CAS No.: 31510-13-1
• Molecular Formula: C₁₄H₁₉NO
• Molecular Weight: 217.311
• Mol file: 31510-13-1.mol

Synonyms:N-cycloheptylbenzamide

Chemical Property of N-cycloheptylbenzamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-CYCLOHEPTYLBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-cycloheptylbenzamide

There total 8 articles about N-cycloheptylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

→ N-cycloheptylbenzamide (31510-13-1)

Guidance literature:

for 15h;

Reference yield: 75.0%

cycloheptane (291-64-5) + benzamide (55-21-0,27208-38-4) → N-cycloheptylbenzamide (31510-13-1)

Guidance literature:

With copper(l) iodide; di-tert-butyl peroxide; 4,7-dimethoxy-1,10-phenanthroline; In 1,2-dichloro-benzene; at 100 ℃; for 36h; Inert atmosphere;

DOI:10.1021/ja411912p

Reference yield: 70.0%

cycloheptanol (502-41-0) + benzonitrile (100-47-0) → N-cycloheptylbenzamide (31510-13-1)

Guidance literature:

cycloheptanol; benzonitrile; With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 15 - 22 ℃; Inert atmosphere;

With thionyl chloride; In dichloromethane; at 20 ℃; stereoselective reaction; Inert atmosphere;

DOI:10.1002/adsc.201300233

upstream raw materials:

cycloheptanamine

benzoyl chloride

2-(2-Methyl-3-oxy-5,6,7,8-tetrahydro-4H-cycloheptaimidazol-1-yl)-cycloheptanone oxime

benzonitrile

Downstream raw materials:

N-methyl-N-<(1S)-4-oxocycloheptyl>benzamide

N-(S)-1,4-Dioxa-spiro[4.6]undec-8-yl-N-methyl-benzamide

(S)-N-(1,4-Dioxa-spiro[4.6]undec-8-yl)-benzamide

N-<(1S)-4-oxocycloheptyl>benzamide