6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

Base Information

Chemical Name:6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione
CAS No.:137476-11-0
Molecular Formula:C₂₆H₄₀N₄O₄
Molecular Weight:472.628
Hs Code.:

Synonyms:6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

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Chemical Property of 6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

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Technology Process of 6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

There total 3 articles about 6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 541-41-3
chloroformic acid ethyl ester

: 137476-10-9
6-amino-1-benzyl-5-(dodecylamino)-2,4-pyrimidinedione

: 137476-11-0
6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1021/jm00062a020

Reference yield:

: 124-22-1
n-Dodecylamine

: 137476-11-0
6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / butan-1-ol / 3 h / Heating

2: 69 percent / K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jm00062a020

Reference yield:

: 72816-87-6
6-amino-1-benzyl-5-bromo-2,4(1H)-pyrimidinedione

: 137476-11-0
6-amino-1-benzyl-5-(N-dodecyl-N-(ethoxycarbonyl)amino)-2,4-pyrimidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / butan-1-ol / 3 h / Heating

2: 69 percent / K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1021/jm00062a020