1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

Base Information

Chemical Name:1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole
CAS No.:265657-42-9
Molecular Formula:C₁₂H₁₃N₇S
Molecular Weight:287.348
Hs Code.:

Synonyms:1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

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Chemical Property of 1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

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Technology Process of 1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

There total 9 articles about 1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₁₂H₁₂N₅OS₂^(1-)*K⁽¹⁺⁾

: 265657-42-9
1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

Guidance literature:: With hydrazine hydrate; In water; for 4h; Heating;

Reference yield:

: 265657-41-8
5-methyl-1-(4-methylphenyl)-1,2,3-triazole-4-carbonylhydrazine

: 265657-42-9
1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 14 h / 20 °C

2: 18 g / hydrazine hydrate / H₂O / 4 h / Heating

With potassium hydroxide; hydrazine hydrate; In ethanol; water;
DOI:10.1081/SCC-100000183

Reference yield:

: 210159-05-0
5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carboxylic acid

: 265657-42-9
1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-1,3,4-triazole

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / conc. H₂SO₄ / 10 h / Heating

2: 91 percent / 85 percent hydrazine hydrate / ethanol / 6 h / Heating

3: potassium hydroxide / ethanol / 14 h / 20 °C

4: 18 g / hydrazine hydrate / H₂O / 4 h / Heating

With potassium hydroxide; sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1081/SCC-100000183