(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

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Chemical Name:(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester
CAS No.:189132-07-8
Molecular Formula:C₃₆H₅₂N₄O₉
Molecular Weight:684.83
Hs Code.:

(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

Synonyms:(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

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Chemical Property of (S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

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Technology Process of (S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

There total 4 articles about (S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13650-73-2
2,5-dioxopyrrolidin-1-yl O-benzyl-N-t-butoxycarbonyl-L-serinate

: 36752-47-3
Lys(Z)-Leu-OMe hydrochloride

: 189132-07-8
(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1021/jm9608671

Reference yield:

: 34404-36-9
Boc-Lys(Z)-OSu

: 189132-07-8
(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

2: 97 percent / 4N aq. HCl / dioxane / 4 h / Ambient temperature

3: 90 percent / Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm9608671

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 189132-07-8
(S)-2-[(S)-2-((S)-3-Benzyloxy-2-tert-butoxycarbonylamino-propionylamino)-6-benzyloxycarbonylamino-hexanoylamino]-4-methyl-pentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

2: 97 percent / 4N aq. HCl / dioxane / 4 h / Ambient temperature

3: 90 percent / Et₃N / CH₂Cl₂ / 16 h / Ambient temperature

With hydrogenchloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jm9608671