triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

Base Information

Chemical Name:triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate
CAS No.:1374964-59-6
Molecular Formula:C₆H₁₅N*C₁₈H₁₄ClNO₂
Molecular Weight:412.959
Hs Code.:

Synonyms:triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

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Chemical Property of triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

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Technology Process of triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

There total 4 articles about triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1374964-58-5
5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylic acid

: 121-44-8
triethylamine

: 1374964-59-6
triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

Guidance literature:: In diethyl ether; at 20 ℃; for 10h;
DOI:10.1021/ml3000462

Reference yield:

: 1374964-71-2
ethyl 5-chloro-3-(1-phenylvinyl)-1H-indole-2-carboxylate

: 1374964-59-6
triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylzinc; trifluoroacetic acid / dichloromethane / 0.33 h / Inert atmosphere

1.2: 2 h / Inert atmosphere

2.1: potassium hydroxide / ethanol; water / 2 h / 80 °C

3.1: diethyl ether / 10 h / 20 °C

With diethylzinc; trifluoroacetic acid; potassium hydroxide; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/ml3000462

Reference yield:

: 1374964-75-6
ethyl 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

: 1374964-59-6
triethylammonium 5-chloro-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water / 2 h / 80 °C

2: diethyl ether / 10 h / 20 °C

With potassium hydroxide; In diethyl ether; ethanol; water;
DOI:10.1021/ml3000462