10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline

Base Information

• Chemical Name: 10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline
• CAS No.: 73323-30-5
• Molecular Formula: C₁₆H₁₂ClN₃
• Molecular Weight: 281.744
• Mol file: 73323-30-5.mol

Synonyms:10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline

Chemical Property of 10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline

There total 1 articles about 10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.6%

1-(1-chloro-5,8-dimethylisoquinolin-6-yl)-1H-v-triazolo<4,5-c>pyridine (73323-31-6) → 10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline (73323-30-5) + 5,11-Dimethyl-dipyrido<4,3-b><3,4-f>indol (65222-36-8)

Guidance literature:

In ethanol; triethylamine; for 87h; Irradiation;

DOI:10.1021/jo01299a028

Reference yield: 48.0%

10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline (73323-30-5) + diethylaminopropylamine (104-78-9) → 10-((γ-(diethylamino)propyl)amino)-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline (73323-33-8)

Guidance literature:

for 4.5h; Heating;

DOI:10.1021/jo01299a028

Reference yield:

10-chloro-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline (73323-30-5) + 1-amino-3-(dimethylamino)propane (109-55-7) → 10-((γ-(dimethylamino)propyl)amino)-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline (73323-34-9)

Guidance literature:

for 4.5h; Heating;

DOI:10.1021/jo01299a028

upstream raw materials:

1-(1-chloro-5,8-dimethylisoquinolin-6-yl)-1H-v-triazolo<4,5-c>pyridine

Downstream raw materials:

10-((γ-(dimethylamino)propyl)amino)-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline

10-((γ-(diethylamino)propyl)amino)-6,11-dimethyl-5H-pyrido<3',4':4,5>pyrrolo<2,3-g>isoquinoline