2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride

Base Information

• Chemical Name: 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride
• CAS No.: 1204301-94-9
• Molecular Formula: C₁₇H₂₅NO₃*ClH
• Molecular Weight: 327.851

Synonyms:2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride

Chemical Property of 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride

Chemical Property:

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Technology Process of 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride

There total 1 articles about 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[3-(4-methoxycarbonyl-3-methylphenoxy)propyl]piperidine-1-carboxylic acid tert-butyl ester (1204301-92-7) → 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride (1204301-94-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 3h;

Reference yield:

2,5-dichloropyrimidine (22536-67-0) + 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride (1204301-94-9) → 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid methyl ester (1204316-03-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 100 ℃; for 16h;

Reference yield:

bromocyane (506-68-3) + 2-methyl-4-(3-piperidin-4-ylpropoxy)-benzoic acid methyl ester hydrochloride (1204301-94-9) → 4-[3-(1-cyanopiperidin-4-yl)propoxy]-2-methylbenzoic acid methyl ester (1204301-93-8)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 0 - 20 ℃;

upstream raw materials:

4-[3-(4-methoxycarbonyl-3-methylphenoxy)propyl]piperidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid methyl ester

4-{3-[1-(5-ethylpyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid methyl ester

4-[3-(1-cyanopiperidin-4-yl)propoxy]-2-methylbenzoic acid methyl ester

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