n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

Base Information

Chemical Name:n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside
CAS No.:471930-59-3
Molecular Formula:C₆₀H₇₆O₁₅
Molecular Weight:1037.25
Hs Code.:

Synonyms:n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

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Technology Process of n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

There total 12 articles about n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 385421-79-4
4-pentenyl 3,6-di-O-benzyl-2-O-pivaloyl-β-D-glucopyranoside

: 471930-54-8
dibutyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranoside phosphate

: 471930-59-3
n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

Guidance literature:: With t-butyldimethylsiyl triflate; In dichloromethane; at -78 - -60 ℃; for 1h;
DOI:10.1021/jo025834+

Reference yield:

: 821-09-0
n-Pent-4-enyl alcohol

: 471930-59-3
n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: TBSOTf / -78 °C

2: hydrazine acetate / CH₂Cl₂; methanol

3: 82 percent / TBSOTf / CH₂Cl₂ / 1 h / -78 - -60 °C

With t-butyldimethylsiyl triflate; hydrazinium monoacetate; In methanol; dichloromethane;
DOI:10.1021/jo025834+

Reference yield:

: 3282-30-2
pivaloyl chloride

: 471930-59-3
n-pentenyl 3,6-dibenzyl-4-levulinoyl-2-pivaloyl-β-D-galactopyranosyl-(1->4)-3,6-dibenzyl-2-pivaloyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 980 mg / DMAP / CH₂Cl₂ / 14 h / 0 °C

2: 82 percent / TBSOTf / CH₂Cl₂ / 1 h / -78 - -60 °C

With dmap; t-butyldimethylsiyl triflate; In dichloromethane;
DOI:10.1021/jo025834+