C₇₅H₉₃N₇O₁₁Si

Base Information

Chemical Name:C₇₅H₉₃N₇O₁₁Si
CAS No.:854443-32-6
Molecular Formula:C₇₅H₉₃N₇O₁₁Si
Molecular Weight:1296.69
Hs Code.:

C<sub>75</sub>H<sub>93</sub>N<sub>7</sub>O<sub>11</sub>Si

Synonyms:C₇₅H₉₃N₇O₁₁Si

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Chemical Property of C₇₅H₉₃N₇O₁₁Si

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Technology Process of C₇₅H₉₃N₇O₁₁Si

There total 18 articles about C₇₅H₉₃N₇O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 854443-31-5
[(1S,2S)-1-(2-{(S)-4-Allyloxycarbonylamino-1-[(S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidine-1-carbonyl]-butylamino}-ethyl)-2-azido-3-(4-benzyloxy-phenyl)-propoxy]-acetic acid tert-butyl ester

: 35661-60-0
Fmoc-Leu-OH

: 854443-32-6
C₇₅H₉₃N₇O₁₁Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tet.2005.03.061

Reference yield:

: 86827-18-1,92455-53-3,16677-29-5
N-benzyloxycarbonyl-O-benzyl-L-tyrosine

: 854443-32-6
C₇₅H₉₃N₇O₁₁Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: isobutyl chloroformate; N-methyl morpholine / CH₂Cl₂ / 0.25 h / -15 °C

1.2: 92 percent / CH₂Cl₂ / 2 h / -15 - 20 °C

2.1: 94 percent / diethyl ether; tetrahydrofuran / -78 °C

3.1: 0.47 g / K-selectride / tetrahydrofuran / 19 h / -78 °C

4.1: 84 percent / aq. KOH / ethanol / 6 h / Heating

5.1: 85 percent / triflyl azide; 4-dimethylaminopyridine; CuSO₄ / CH₂Cl₂ / 2 h / 20 °C

6.1: tetrabutylammonium hydrogensulfate; aq. NaOH / benzene / 1.5 h / 20 °C

7.1: 0.832 g / osmium tetroxide; 4-methylmorpholine N-oxide / tetrahydrofuran; H₂O; acetone / 2.5 h / 20 °C

8.1: 88 percent / lead tetraacetate; Na₂CO₃ / benzene / 1.17 h / 0 - 20 °C

9.1: 95 percent / sodium triacetoxyborohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.1: 52 percent / diisopropylethylamine; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆ / dimethylformamide / 24 h / 0 - 20 °C

With 4-methyl-morpholine; lead(IV) acetate; dmap; potassium hydroxide; sodium hydroxide; osmium(VIII) oxide; triflic azide; tetra(n-butyl)ammonium hydrogensulfate; sodium tris(acetoxy)borohydride; sodium carbonate; potassium tri-sec-butyl-borohydride; copper(II) sulfate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; HATU; isobutyl chloroformate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; benzene; 2.1: Grignard reaction;
DOI:10.1016/j.tet.2005.03.061

Reference yield:

: 854443-24-6
(S)-2-benzyloxycarbonylamino-1-(4-benzyloxyphenyl)-hex-5-en-3-one

: 854443-32-6
C₇₅H₉₃N₇O₁₁Si

Guidance literature:: Multi-step reaction with 8 steps

1: 0.47 g / K-selectride / tetrahydrofuran / 19 h / -78 °C

2: 84 percent / aq. KOH / ethanol / 6 h / Heating

3: 85 percent / triflyl azide; 4-dimethylaminopyridine; CuSO₄ / CH₂Cl₂ / 2 h / 20 °C

4: tetrabutylammonium hydrogensulfate; aq. NaOH / benzene / 1.5 h / 20 °C

5: 0.832 g / osmium tetroxide; 4-methylmorpholine N-oxide / tetrahydrofuran; H₂O; acetone / 2.5 h / 20 °C

6: 88 percent / lead tetraacetate; Na₂CO₃ / benzene / 1.17 h / 0 - 20 °C

7: 95 percent / sodium triacetoxyborohydride / 1,2-dichloro-ethane / 1 h / 20 °C

8: 52 percent / diisopropylethylamine; O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium PF₆ / dimethylformamide / 24 h / 0 - 20 °C

With lead(IV) acetate; dmap; potassium hydroxide; sodium hydroxide; osmium(VIII) oxide; triflic azide; tetra(n-butyl)ammonium hydrogensulfate; sodium tris(acetoxy)borohydride; sodium carbonate; potassium tri-sec-butyl-borohydride; copper(II) sulfate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/j.tet.2005.03.061