acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

Base Information

Chemical Name:acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester
CAS No.:329349-91-9
Molecular Formula:C₂₂H₂₉NO₄Si
Molecular Weight:399.562
Hs Code.:

acetic acid 2-[4-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

Synonyms:acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

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Chemical Property of acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

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Technology Process of acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

There total 1 articles about acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131230-76-7
4-[(tert-butyldimethylsilyloxy)methyl]aniline

: 5538-51-2
O-acetylsalicyloyl chloride

: 329349-91-9
acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 0.333333h;
DOI:10.1002/1521-3773(20010105)40:1<207::AID-ANIE207>3.0.CO;2-K DOI:10.1021/ja012125p

Reference yield: 43.0%

: 329349-91-9
acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

: 329349-92-0
acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-3,6-dioxo-cyclohexa-1,4-dienylcarbamoyl]-phenyl ester

Guidance literature:: With water; Dess-Martin periodane; In dichloromethane; at 25 ℃; for 3h;
DOI:10.1002/1521-3773(20010105)40:1<207::AID-ANIE207>3.0.CO;2-K

Reference yield:

: 329349-91-9
acetic acid 2-[4-(tert-butyl-dimethyl-silanyloxymethyl)-phenylcarbamoyl]-phenyl ester

: 175448-32-5
epoxyquinomycin B

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / Dess-Martin periodinane; H₂O / CH₂Cl₂ / 6 h / 25 °C

2: 100 percent / H₂O₂; K₂CO₃ / tetrahydrofuran; H₂O / 0.5 h / 25 °C

3: 95 percent / HF*py / tetrahydrofuran / 0.17 h / 20 °C

With water; dihydrogen peroxide; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja012125p