4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Base Information

Chemical Name:4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride
CAS No.:1118916-80-5
Molecular Formula:C₂₃H₂₉N₂*Cl
Molecular Weight:368.95
Hs Code.:

Synonyms:4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Suppliers and Price of 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Chemical Property:

Purity/Quality:: HPLC≥98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

There total 4 articles about 4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 75105-48-5
N,N'-dimesitylformamidine

: 4091-39-8
3-chloro-2-butanone

: 1118916-80-5
4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Guidance literature:: N,N'-dimesitylformamidine; 3-chloro-2-butanone; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 110 ℃; for 20h;

With hydrogenchloride; acetic anhydride; In water; toluene; at 90 ℃; for 13.5h;

Reference yield:

: C₂₃H₃₁N₂O⁽¹⁺⁾*Cl^(1-)

: 1118916-80-5
4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Guidance literature:: With hydrogenchloride; acetic anhydride; In water; toluene; at 90 ℃; for 13.5h;
DOI:10.1021/ol8029609

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 1118916-80-5
4,5-dimethyl-1,3-bis-(2,4,6-trimethylphenyl)-3H-imidazol-1-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / neat (no solvent) / 3 h / 160 °C

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 110 °C

2.2: 15 h / 90 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; In acetonitrile;
DOI:10.1021/ja511622e