hexamethylcyclotrigermatrithiane

Base Information

Chemical Name:hexamethylcyclotrigermatrithiane
CAS No.:16090-54-3
Molecular Formula:C₆H₁₈Ge₃S₃
Molecular Weight:404.177
Hs Code.:

Synonyms:hexamethylcyclotrigermatrithiane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexamethylcyclotrigermatrithiane

Chemical Property:

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Technology Process of hexamethylcyclotrigermatrithiane

There total 6 articles about hexamethylcyclotrigermatrithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 62827-97-8
Bis(trimethylsilyl)thioketene

: 76054-64-3
7,7-dimethyl-1,4,5,6-tetraphenyl-2,3-benzo-7-germanorbornadiene

: ((CH₃)3Si)2C(CSGe₂)(CH₃)4

: 751-38-2
1,2,3,4-tetraphenylnaphthalene

: 16090-54-3
hexamethylcyclotrigermatrithiane

: 14630-40-1
Bis(trimethylsilyl)ethyne

Guidance literature:: In benzene; all manipulations under dry Ar; heating benzene soln. of 2,3-benzo-7,7-dimethyl-1,4,5,6-tetraphenyl-7-germanorborna-2,5-diene and bis(trimethylsilyl)thioketene (70°C, 3 h); preparative GLC (10% SF-96 on Celite 545);
DOI:10.1021/om00108a016

Reference yield: 80.0%

: Pt(((C₆H₅)2PCH₂)2)(S(Ge(CH₃)2)2)

: 7726-95-6
bromine

: 74-88-4
methyl iodide

: 1730-66-1
methylgermanium bromide

: 6199-00-4
Hexamethyldigermaniumsulfid

: 16090-54-3
hexamethylcyclotrigermatrithiane

Guidance literature:: In benzene; Ar or N2-atmosphere, 20°C;

Reference yield: 37.0%

: 98187-54-3
2,2,4,4,6,6,8,8-octamethyl-1,5,2,4,6,8-dithiatetragermocane

: 1450-31-3
Thiobenzophenon

: 530-48-3
1,1-Diphenylethylene

: 16090-54-3
hexamethylcyclotrigermatrithiane

Guidance literature:: In neat (no solvent); (Ar); thermolysis of Ge compd. in presence of Ph2CS at 230°C for14 h; not isolated, detected by chromy.;
DOI:10.1016/0022-328X(85)87190-4