N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

Base Information

Chemical Name:N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride
CAS No.:1379662-58-4
Molecular Formula:C₃₃H₄₃N₈O₂*Cl
Molecular Weight:619.21
Hs Code.:

Synonyms:N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

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Chemical Property of N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

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Technology Process of N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

There total 5 articles about N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1379662-55-1
1,4-bis[2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl]-1,4-diazabuta-1,3-diene

: 1379662-58-4
N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

Guidance literature:: With chloro-trimethyl-silane; In tetrahydrofuran; at 40 ℃;
DOI:10.1039/c2dt30249g

Reference yield:

: 1379662-49-3
4-azido-2,6-diisopropylaniline

: 1379662-58-4
N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / methanol; water / 4 h / 20 °C

2: [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)] / methanol; ethyl acetate / 72 h / 30 °C

3: chloro-trimethyl-silane / tetrahydrofuran / 40 °C

With chloro-trimethyl-silane; [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)]; acetic acid; In tetrahydrofuran; methanol; water; ethyl acetate;
DOI:10.1039/c2dt30249g

Reference yield:

: 1379662-50-6
1,4-bis(4-azido-2,6-diisopropylphenyl)-1,4-diazabuta-1,3-diene

: 1379662-58-4
N,N'-bis(2,6-diisopropyl-4-(4-hydroxymethyl-1,2,3-1H-triazol-1-yl)phenyl)imidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)] / methanol; ethyl acetate / 72 h / 30 °C

2: chloro-trimethyl-silane / tetrahydrofuran / 40 °C

With chloro-trimethyl-silane; [Cu(4,7-dichloro-1,10-phenanthroline)(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)]; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1039/c2dt30249g