N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine

Base Information

• Chemical Name: N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine
• CAS No.: 93725-68-9
• Molecular Formula: C₁₇H₂₃N₃S
• Molecular Weight: 301.456

Synonyms:N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine

Chemical Property of N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine

Chemical Property:

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Technology Process of N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine

There total 3 articles about N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

N,N-dimethyl-N'-(pyridine-2-yl)ethane-1,2-diamine (23826-72-4) → N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine (93725-68-9)

Guidance literature:

N,N-dimethyl-N'-(pyridine-2-yl)ethane-1,2-diamine; With lithium amide; In acetonitrile; for 0.0833333h; Inert atmosphere;

4-methylthiobenzyl halide; In acetonitrile; for 8h; Inert atmosphere; Reflux;

DOI:10.1016/j.ejmech.2014.04.041

Reference yield:

2-chloropyridine (109-09-1) → N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine (93725-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 12 h / 140 °C / Inert atmosphere; Sealed tube

2.1: lithium amide / acetonitrile / 0.08 h / Inert atmosphere

2.2: 8 h / Inert atmosphere; Reflux

With lithium amide; In acetonitrile;

DOI:10.1016/j.ejmech.2014.04.041

Reference yield:

→ N-[(4-methylthiophenyl)methyl]-N-[2-(dimethylamino)ethyl]pyridin-2-amine (93725-68-9)

Guidance literature:

2-<4-Methylmercaptobenzylamino>-pyridin, 1. NaNH2, 2. <2-Chlorethyl>-dimethylamin;

upstream raw materials:

2-chloropyridine

N,N-dimethyl-N'-(pyridine-2-yl)ethane-1,2-diamine

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