6-<4-benzoyl>hexanoic acid

Base Information

Chemical Name:6-<4-benzoyl>hexanoic acid
CAS No.:125174-06-3
Molecular Formula:C₁₇H₂₃Cl₂NO₃
Molecular Weight:360.281
Hs Code.:

6-<4-<N,N-bis(2-chloroethyl)amino>benzoyl>hexanoic acid

Synonyms:6-<4-benzoyl>hexanoic acid

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Chemical Property of 6-<4-benzoyl>hexanoic acid

Chemical Property:

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Technology Process of 6-<4-benzoyl>hexanoic acid

There total 5 articles about 6-<4-benzoyl>hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125174-05-2
7-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-7-oxo-heptanoic acid methyl ester

: 125174-06-3
6-<4-benzoyl>hexanoic acid

Guidance literature:: With hydrogenchloride; at 80 ℃; for 1h; Yield given;
DOI:10.1021/jm00166a015

Reference yield:

: 125174-01-8
6-(4-aminobenzoyl)hexanoic acid

: 125174-06-3
6-<4-benzoyl>hexanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / H₂SO₄

2: 38 percent / acetic acid; tetrahydrofuran / 168 h / 20 °C

3: Et₃N / CH₂Cl₂ / 3 h / 20 °C

4: NaCl / dimethylformamide / 0.08 h / Heating

5: conc. HCl / 1 h / 80 °C

With hydrogenchloride; sulfuric acid; triethylamine; sodium chloride; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00166a015

Reference yield:

: 125174-00-7
2-(4-Amino-benzoyl)-cyclohexanone

: 125174-06-3
6-<4-benzoyl>hexanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 61 percent / KOH, H₂O / 1.25 h / Heating

2: 87 percent / H₂SO₄

3: 38 percent / acetic acid; tetrahydrofuran / 168 h / 20 °C

4: Et₃N / CH₂Cl₂ / 3 h / 20 °C

5: NaCl / dimethylformamide / 0.08 h / Heating

6: conc. HCl / 1 h / 80 °C

With hydrogenchloride; potassium hydroxide; sulfuric acid; water; triethylamine; sodium chloride; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00166a015