N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

Base Information

Chemical Name:N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate
CAS No.:1620644-87-2
Molecular Formula:C₈HCl₂N₂O₂*C₃₁H₃₁N₂O₄
Molecular Weight:723.612
Hs Code.:

Synonyms:N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

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Chemical Property of N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

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Technology Process of N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

There total 5 articles about N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1620644-83-8
N-[2-(3-acetyl-1-benzyl-4H-pyridin-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 1620644-87-2
N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

Guidance literature:: In acetonitrile; at 20 ℃;

Reference yield:

: 1620646-06-1
N-but-3-enyl-3,4-dimethoxy-N-phenyl-benzamide

: 1620644-87-2
N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

Guidance literature:: Multi-step reaction with 3 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C / Inert atmosphere

2: scandium tris(trifluoromethanesulfonate); sodium sulfate / dichloromethane / 48 h / 20 °C

3: acetonitrile / 20 °C

With Hoveyda-Grubbs catalyst second generation; sodium sulfate; scandium tris(trifluoromethanesulfonate); In dichloromethane; acetonitrile;

Reference yield:

: 100-46-9
benzylamine

: 1620644-87-2
N-[2-(3-acetyl-1-benzyl-pyridin-1-ium-4-yl)ethyl]-3,4-dimethoxy-N-phenyl-benzamide 2,3-dichloro-5,6-dicyano-4-oxo-cyclohex-1,5-dien-1-olate

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 20 °C

2: scandium tris(trifluoromethanesulfonate); sodium sulfate / dichloromethane / 48 h / 20 °C

3: acetonitrile / 20 °C

With sodium sulfate; scandium tris(trifluoromethanesulfonate); In dichloromethane; chloroform; acetonitrile;