Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Base Information

Chemical Name:Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)
CAS No.:80715-08-8
Molecular Formula:C₄₆H₅₂N₂O₄
Molecular Weight:696.93
Hs Code.:

Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Synonyms:Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

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Chemical Property of Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

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Technology Process of Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

There total 4 articles about Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 917-64-6
methyl magnesium iodide

: 80715-06-6
Ethandiyl-1-(3-benzyl-8-hydroxy-5-oxo-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-hydroxy-5-oxo-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

: 80715-08-8
Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Guidance literature:: In diethyl ether; benzene; for 5h; Heating;
DOI:10.1002/ardp.19813141205

Reference yield:

: 41276-30-6
C₉H₁₄O₃NC₆H₅

: 80715-08-8
Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 1.) 80percent H₂SO₄, 2.) 10percent aq. NaHCO₃ / 1.) room temp., 3 days, 2.) acetone, room temp., 20 h

2: 17 percent / diethyl ether; benzene / 5 h / Heating

With sulfuric acid; sodium hydrogencarbonate; In diethyl ether; benzene;
DOI:10.1002/ardp.19813141205

Reference yield:

: 4721-07-7,29700-22-9
oxyresveratrol

: 80715-08-8
Ethandiyl-1-(3-benzyl-8-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-9-pyridin)-2-(3-benzyl-10-methoxy-5,5-dimethyl-1,2,3,4-tetrahydro-5H-benzopyrano-<3,4-c>-8-pyridin)

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C

2: 68 percent / 1.) 80percent H₂SO₄, 2.) 10percent aq. NaHCO₃ / 1.) room temp., 3 days, 2.) acetone, room temp., 20 h

3: 17 percent / diethyl ether; benzene / 5 h / Heating

With sulfuric acid; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In diethyl ether; benzene;
DOI:10.1002/ardp.19813141205